Methylamine → HCID 70636802, 화합물
반응식
O=[C:2]1[CH2:20][CH2:19][N:5]2[C:6]3[CH:18]=[CH:17][CH:16]=[CH:15][C:7]=3[CH2:8][C:9]3[CH:14]=[CH:13][CH:12]=[CH:11][C:10]=3[CH:4]2[CH2:3]1.[CH3:21][NH2:22].[H][H]>C(O)C.[Pd]>[CH3:21][NH:22][CH:2]1[CH2:20][CH2:19][N:5]2[C:6]3[CH:18]=[CH:17][CH:16]=[CH:15][C:7]=3[CH2:8][C:9]3[CH:14]=[CH:13][CH:12]=[CH:11][C:10]=3[CH:4]2[CH2:3]1참가 물질
6
실험 절차
1 g of 2-keto-1,2,3,4,10,14b-hexahydro-pyridino[ 1,2-a] -dibenzo[c,f]-azepine is dissolved in 100 ml of ethanol, after which 10 ml of methylamine and 200 mg of palladium (10%) on charcoal are added. Then hydrogen is passed through this mixture until no hydrogen is absorbed any longer.
후처리
- customis absorbed any longer
출처 및 근거
- ORD 기록
- ord-5f188c07518941e78f7cf37727122b26
- 출처 데이터셋
- uspto-grants-1977_10
- 특허 번호
- US04054572
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