Aminoethylpiperazine → (3-Chloropropanoyl)urea

HRID 973134

반응식

HRID 973134 반응식
[NH2:1]CCN1CCNCC1.[Cl:10][CH2:11][CH2:12][C:13]([N:15]=[C:16]=[O:17])=[O:14]>>[Cl:10][CH2:11][CH2:12][C:13]([NH:15][C:16]([NH2:1])=[O:17])=[O:14]

참가 물질

3

반응물 2

HCID 8795AminoethylpiperazineHCID 135723743-Chloropropanoyl isocyanate

생성물 1

HCID 12937417(3-Chloropropanoyl)urea수율 263%

실험 절차

In the same way, reaction of 6.5 g (50 mmols) of N-(2-aminoethyl)piperazine with 14.3 g (106 mmols) of 3-chloropropionyl isocyanate gives a quantitative yield of 19.8 g of the 3-chloropropionyl urea of the formula ##STR10## Melting point: 125°-130° C.

출처 및 근거

ORD 기록
ord-1d934c9c935a41dea3f3940d8c0f79b1
출처 데이터셋
uspto-grants-1977_10
특허 번호
US04055431

연결된 노트

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