p-Cyclohexyl-alpha-methylbenzylamine hydrochloride → 2-(rho-Cyclohexyl-alpha-methylbenzylimino)hexahydroazepine hydrochloride
반응식
[ClH:1].[CH:2]1([C:8]2[CH:16]=[CH:15][C:11]([CH:12]([NH2:14])[CH3:13])=[CH:10][CH:9]=2)[CH2:7][CH2:6][CH2:5][CH2:4][CH2:3]1.Cl.C[CH:19]([NH2:34])[C:20]1C=[CH:24][C:23](CCC2C=CC=CC=2)=[CH:22][CH:21]=1>>[ClH:1].[CH:2]1([C:8]2[CH:9]=[CH:10][C:11]([CH:12]([N:14]=[C:19]3[CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][NH:34]3)[CH3:13])=[CH:15][CH:16]=2)[CH2:3][CH2:4][CH2:5][CH2:6][CH2:7]1참가 물질
3
실험 절차
Following essentially the same procedure described in Example IV above and substituting ρ-cyclohexyl-α-methylbenzylamine hydrochloride for the α-methyl-ρ-phenyethylbenzylamine hydrochloride above, results in the formation of 2-(ρ-cyclohexyl-α-methylbenzylimino)hexahydroazepine hydrochloride having a M.P. of 245°-7° C.
출처 및 근거
- ORD 기록
- ord-f765477b29c84d9bbbdc6becef562af2
- 출처 데이터셋
- uspto-grants-1977_10
- 특허 번호
- US04055561
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