Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-Hexanol → Hexyl 2-hydroxy-2-methylpropanoate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-Hexanol | HCID 8103 | — |
| 반응물 | Propanamide, 2-hydroxy-2-methyl- | HCID 83059 | — |
| 생성물 | Hexyl 2-hydroxy-2-methylpropanoate | HCID 21401559 | 51.8% |
반응 단계
A mixture of 20.6 g of α-hydroxy-isobutyramide and 204 g of n-hexyl alcohol was heated in the presence of 0.45 g of PbO for 6 hours at 200° C. in an autoclave. On working up by distillation, 19.5 g (= 51.8 percent of theory) of α-hydroxy-isobutyric acid-n-hexyl-ester were obtained. The amide conversion is 75 percent.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04055590 |
| 출처 데이터셋 | uspto-grants-1977_10 |
| ORD ID | ord-cd14d858d59547409c78185637444a00 |
| 출처 메모 | uspto-grants-1977_10 |