Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sodium Hydroxide → 4-Methylhexylmethylmalonic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 반응물 | Diethyl 4-methylhexylmethylmalonate | HCID 54113602 | — |
| 용매 | Methanol | HCID 887 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | 4-Methylhexylmethylmalonic acid | HCID 54000156 | — |
반응 단계
First, 8.18 g (0.22 mol) of sodium hydroxide was dissolved in a mixture solution of 28 ml of water and 14 ml of methanol, thus forming a solution. Next, g of the crude product (II), not refined, was added to the resultant solution and reacted with the solution at 20° C. for three to five hours, thereby obtaining 18.4 g of 4-methylhexylmethylmalonic acid (III). This reaction is represented as follows: ##STR4##
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05063058 |
| 출처 데이터셋 | uspto-grants-1991_11 |
| ORD ID | ord-940c9a4c925c424b8d6bdebca07d15d3 |
| 출처 메모 | uspto-grants-1991_11 |