Thionyl Chloride → [3-(Trifluoromethyl)phenoxy]acetyl chloride
반응식
[F:1][C:2]([F:15])([F:14])[C:3]1[CH:4]=[C:5]([CH:11]=[CH:12][CH:13]=1)[O:6][CH2:7][C:8](O)=[O:9].S(Cl)([Cl:18])=O>>[F:1][C:2]([F:15])([F:14])[C:3]1[CH:4]=[C:5]([CH:11]=[CH:12][CH:13]=1)[O:6][CH2:7][C:8]([Cl:18])=[O:9]참가 물질
3
실험 절차
A solution of 6 g of the product of Step B in 36 ml of thionyl chloride was refluxed with stirring for one hour and was evaporated to dryness under reduced pressure to obtain 6.44 g of the desired product which was used as is for the next step.
후처리
- customwas evaporated to dryness under reduced pressure
출처 및 근거
- ORD 기록
- ord-c09db5187a1f4a44a6e4420e23b35327
- 출처 데이터셋
- uspto-grants-1991_11
- 특허 번호
- US05064861
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