Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrochloric Acid → Methyl 3-(4,6-bis(trichloromethyl)-s-triazin-2-yl)benzoate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | Trichloroacetonitrile | HCID 11011 | — |
| 반응물 | Benzoic acid, 3-cyano-, methyl ester | HCID 83554 | — |
| 반응물 | Bromhydrol | HCID 166749 | — |
| 생성물 | Methyl 3-(4,6-bis(trichloromethyl)-s-triazin-2-yl)benzoate | HCID 14572905 | — |
반응 단계
Methyl 3-cyanobenzoate (70 pw) are mixed with trichloroacetonitrile (376 pw) and aluminum bromide (13.9 pw) as described in Example 1, step 2, hydrogen chloride gas is added, the mixture is allowed to react and the reaction product is separated. Recrystallization from ethanol gives 160 pw=82% of white crystals of methyl 3-(4,6-bis(trichloromethyl)-s-triazin-2-yl)benzoate. M.p.: 115 to 117° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05064959 |
| 출처 데이터셋 | uspto-grants-1991_11 |
| ORD ID | ord-75d789af17cf41cba765527cdb44a27a |
| 출처 메모 | uspto-grants-1991_11 |