Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Benzaldehyde → N-Benzylidene-2,4-difluorobenzylamine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Benzaldehyde | HCID 240 | — |
| 반응물 | Water | HCID 962 | — |
| 반응물 | 2,4-Difluorobenzylamine | HCID 2733244 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | N-Benzylidene-2,4-difluorobenzylamine | HCID 19986446 | — |
반응 단계
50.2 g (0.35 mol) of 2,4-difluorobenzylamine and 37.1 g (0.35 mol) of benzaldehyde are dissolved in 140 ml of toluene and heated to reflux. The water produced is separated off using a water separator. The reaction is complete (GC check) after two hours. The solution is evaporated on a vacuum rotary evaporator. 78.9 g (97% of theory) of a slightly yellow liquid are obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05068371 |
| 출처 데이터셋 | uspto-grants-1991_11 |
| ORD ID | ord-6267607942ce40488e1d03f6daa5f76d |
| 출처 메모 | uspto-grants-1991_11 |