참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | 3,7-Dimethyl-1-octanol | HCID 7792 | — |
| 반응물 | Phosphorus tribromide | HCID 24614 | — |
| 용매 | Hexane | HCID 8058 | — |
| 생성물 | 1-Bromo-3,7-dimethyloctane | HCID 137914 | — |
반응 단계
To neat 3,7-dimethyloctanol (5 ml) was added phosphorus tribromide (1.01 ml). The mixture was stirred for 4 hours at 60° C. The reaction mixture was added to a mixture of water and n-hexane. The organic layer was separated and dried over magnesium sulfate. The magnesium sulfate was filtered off, and the filtrate was evaporated under reduced pressure to give 3,7-dimethyloctyl bromide (4.40 g).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | USH0001638 |
|---|
| 출처 데이터셋 | uspto-grants-1997_03 |
|---|
| ORD ID | ord-3494bf0f116242de84cf8586d6e3cba3 |
|---|
| 출처 메모 | uspto-grants-1997_03 |
|---|
