Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Cyclohexane → 3-Trifluoromethyl-2-(2-aminophenylthio)benzonitrile
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Cyclohexane | HCID 8078 | — |
| 반응물 | 2-Aminothiophenol | HCID 8713 | — |
| 반응물 | 2-Fluoro-3-(trifluoromethyl)benzonitrile | HCID 518974 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 생성물 | 3-Trifluoromethyl-2-(2-aminophenylthio)benzonitrile | HCID 19969445 | — |
반응 단계
Using a procedure analagous to that of Example 3(a), 2-aminothiophenol (6.26 g, 50 mmol) was combined with 3-trifluoromethyl-2-fluorobenzonitrile (1 eq) in DMF solvent (50 ml) to give the title compound as a white solid from cyclohexane (10.41 g).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05607929 |
| 출처 데이터셋 | uspto-grants-1997_03 |
| ORD ID | ord-5ea13c82a1fe4e9fb68e4b02a5c661d9 |
| 출처 메모 | uspto-grants-1997_03 |