3-Bromothiophene → 1-(3,5-Dimethyl-4-isoxazolyl)-1-(3-thienyl)ethanol

HRID 975066노트

반응식

HRID 975066 반응식
[C:1]([C:4]1[C:5]([CH3:10])=[N:6][O:7][C:8]=1[CH3:9])(=[O:3])[CH3:2].Br[C:12]1[CH:16]=[CH:15][S:14][CH:13]=1>>[CH3:10][C:5]1[C:4]([C:1]([C:12]2[CH:16]=[CH:15][S:14][CH:13]=2)([OH:3])[CH3:2])=[C:8]([CH3:9])[O:7][N:6]=1

참가 물질

3

반응물 2

HCID 133833-BromothiopheneHCID 127203171-(3,5-Dimethylisoxazol-4-yl)ethanone

생성물 1

HCID 189362861-(3,5-Dimethyl-4-isoxazolyl)-1-(3-thienyl)ethanol

실험 절차

The title compound was prepared following the general method of Example 4 but starting with 4-acetyl-3,5-dimethylisoxazole and 3-bromothiophene. M.p. 93.5°-95° C.

출처 및 근거

ORD 기록
ord-73361ddd1a4d4dab8a837cb8a7040f81
출처 데이터셋
uspto-grants-1997_03
특허 번호
US05607956

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