Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methanol → 3-Methoxy-3-oxo-2-phenylpropanoic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methanol | HCID 887 | — |
| 반응물 | Boron trifluoride etherate | HCID 8000 | — |
| 반응물 | Phenylmalonic acid | HCID 75791 | — |
| 생성물 | 3-Methoxy-3-oxo-2-phenylpropanoic acid | HCID 2817775 | — |
반응 단계
A mixture of phenylmalonic acid (3.6 g, 0.02 mol), boron trifluoride etherate (2.4 mL, 0.02 mol) and 0.8 mL of anhydrous methanol (0.02 mol) was refluxed and stirred for 24 hours. After cooling to room temperature, the reaction mixture was filtered and 20 mL of water was added.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05610188 |
| 출처 데이터셋 | uspto-grants-1997_03 |
| ORD ID | ord-9ce6dd16fcca45f9ab3aea345993b2d6 |
| 출처 메모 | uspto-grants-1997_03 |