Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3-(Methylthio)phenyl isocyanate → 1-Cyclohexyl-1-hydroxy-3-[3-(methylthio)phenyl]urea
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3-(Methylthio)phenyl isocyanate | HCID 141418 | — |
| 반응물 | N-Cyclohexylhydroxylamine hydrochloride | HCID 3084432 | — |
| 생성물 | 1-Cyclohexyl-1-hydroxy-3-[3-(methylthio)phenyl]urea | HCID 19967393 | 27.1% |
반응 단계
Using the general method used to prepare Compound 1, N-(cyclohexyl)hydroxylamine hydrochloride (1.5 g, 10 mmol) was reacted with 3-(methylthio)phenyl isocyanate (1.6 g, 10 mmol) to provide 0.76 g of the desired product as a white solid m.p. 147.2°-147.7° C. Analysis: Calculated for C14H20N2O2S: %C, 59.97; %H, 7.19; %N, 9.99; Found: %C, 60.16; %H, 6.95; %N, 9.96.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05612377 |
| 출처 데이터셋 | uspto-grants-1997_03 |
| ORD ID | ord-124a20a7d7d74e86aa486b16c45b5783 |
| 출처 메모 | uspto-grants-1997_03 |