2-Bromopentane → 1-Benzyloxy-1-(1-methylbutyl)-3-phenylurea

HRID 976637

반응식

Br[CH:2]([CH2:4][CH2:5][CH3:6])[CH3:3].[CH2:7]([O:14][NH:15][C:16]([NH:18][C:19]1[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=1)=[O:17])[C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1>>[CH2:7]([O:14][N:15]([CH:2]([CH3:3])[CH2:4][CH2:5][CH3:6])[C:16]([NH:18][C:19]1[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=1)=[O:17])[C:8]1[CH:9]=[CH:10][CH:11]=[CH:12][CH:13]=1

참가 물질

반응물 2

HCID 78902-Bromopentane

HCID 2542991-(Benzyloxy)-3-phenylurea

생성물 1

HCID 199674041-Benzyloxy-1-(1-methylbutyl)-3-phenylurea수율 67.8%

실험 절차

Using the general method of Compound 42 Part B, 2-bromopentane (2.7 mL, 21.7 mmole) was reacted with 1-benzyloxy-3-phenylurea (4.9 g, 20.1 mmole) to provide 4.26 g of 1-benzyloxy-1-(1-methylbutyl)-3-phenylurea as a yellow oil.

출처 및 근거

ORD 기록: ord-7c65b66eb0234a609b4ed0ca333eec8a
출처 데이터셋: uspto-grants-1997_03
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US05612377

연결된 노트

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