3-Bromohexane → 1-Benzyloxy-1-(1-ethylbutyl)-3-phenylurea

HRID 976640

반응식

HRID 976640 반응식
Br[CH:2]([CH2:5][CH2:6][CH3:7])[CH2:3][CH3:4].[CH2:8]([O:15][NH:16][C:17]([NH:19][C:20]1[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=1)=[O:18])[C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1>>[CH2:8]([O:15][N:16]([CH:2]([CH2:3][CH3:4])[CH2:5][CH2:6][CH3:7])[C:17]([NH:19][C:20]1[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=1)=[O:18])[C:9]1[CH:10]=[CH:11][CH:12]=[CH:13][CH:14]=1

참가 물질

3

반응물 2

HCID 188063-BromohexaneHCID 2542991-(Benzyloxy)-3-phenylurea

생성물 1

HCID 199673721-Benzyloxy-1-(1-ethylbutyl)-3-phenylurea수율 34.5%

실험 절차

Using the general method of Compound 42 Part B, 3-bromohexane (4.59 mL, 32.6 mmole) was reacted with 1-benzyloxy-3-phenylurea (7.3 g, 30.2 mmole) to provide 3.4 g of 1-benzyloxy-1-(1-ethylbutyl)-3-phenylurea.

출처 및 근거

ORD 기록
ord-1fcce69637be4180a82f947abc5b77d3
출처 데이터셋
uspto-grants-1997_03
특허 번호
US05612377

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