참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Thiazolidinedione | HCID 5437 | — |
| 반응물 | Piperidine | HCID 8082 | — |
| 반응물 | 3-Chloro-4,5-dihydroxybenzaldehyde | HCID 2468182 | — |
| 용매 | Acetic Acid | HCID 176 | — |
| 생성물 | 5-[(3,4-Dihydroxy-5-chlorophenyl)methylidene]-thiazolidin-2,4-dione | HCID 54030399 | — |
반응 단계
A solution containing 1.33 g of thiazolidine-2,4-dione, 1.72 g of 3,4-dihydroxy-5-chlorobenzaldehyde and 2 ml of piperidine in 20 ml of acetic acid was heated for five hours at 100° C. Yield 1.9 g (70%), mp 299°-301° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US05614541 |
|---|
| 출처 데이터셋 | uspto-grants-1997_03 |
|---|
| ORD ID | ord-c1768ea405654a8791ddf262b4ba31d8 |
|---|
| 출처 메모 | uspto-grants-1997_03 |
|---|
