Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methyl 4-[2-(5-methyl-2-phenyl-4-oxazolyl)ethyl]benzoate → 4-[2-(5-Methyl-2-phenyl-4-oxazolyl)ethyl]benzyl alcohol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methyl 4-[2-(5-methyl-2-phenyl-4-oxazolyl)ethyl]benzoate | HCID 19965620 | — |
| 반응물 | Aluminium lithium hydride | HCID 21226445 | — |
| 생성물 | 4-[2-(5-Methyl-2-phenyl-4-oxazolyl)ethyl]benzyl alcohol | HCID 54568002 | — |
반응 단계
Methyl 4-[2-(5-methyl-2-phenyl-4-oxazolyl)ethyl]benzoate was reduced with lithium aluminum hydride in the same manner as in Reference Example 12 to yield 4-[2-(5-methyl-2-phenyl-4-oxazolyl)ethyl]benzyl alcohol, which was then recrystallized from ethyl acetate-hexane to yield colorless plates having a melting point of 103°-104° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05614544 |
| 출처 데이터셋 | uspto-grants-1997_03 |
| ORD ID | ord-75b253952b1443f8887904166dc53a19 |
| 출처 메모 | uspto-grants-1997_03 |