Bromine → HCID 13849524, 화합물

HRID 978113노트

반응식

HRID 978113 반응식
[OH:1][C:2]1[CH:16]=[CH:15][C:5]2[C:6]([CH3:14])=[C:7]([C:9]([O:11][CH2:12][CH3:13])=[O:10])[O:8][C:4]=2[CH:3]=1.[Br:17]Br>C(Cl)Cl>[Br:17][C:3]1[C:4]2[O:8][C:7]([C:9]([O:11][CH2:12][CH3:13])=[O:10])=[C:6]([CH3:14])[C:5]=2[CH:15]=[CH:16][C:2]=1[OH:1]

참가 물질

4

반응물 2

HCID 24408BromineHCID 15560986Ethyl 6-hydroxy-3-methyl-2-benzofurancarboxylate

생성물 1

HCID 13849524HCID 13849524, 화합물

시약·촉매·용매 1

HCID 6344Dichloromethane용매2회

실험 절차

A suspension of ethyl 6-hydroxy-3-methylbenzofuran-2-carboxylate (220 mg, 1 mmole) in methylene chloride (6 ml) was treated very slowly with a solution of bromine (160 mg, 1 mmole) in methylene chloride (4 ml) and with efficient stirring.

출처 및 근거

ORD 기록
ord-4c36afc1038a44c88d154e1ef369fc97
출처 데이터셋
uspto-grants-1987_05
특허 번호
US04663347

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