Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3,4-Dichloroaniline → 5-Chloro-3-(3,4-dichlorophenyl)-4-thiazolidinone
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3,4-Dichloroaniline | HCID 7257 | — |
| 반응물 | Thionyl Chloride | HCID 24386 | — |
| 반응물 | 3-(3,4-Dichlorophenyl)-1,3-thiazolidin-4-one | HCID 4585437 | — |
| 반응물 | Thiazolidinone | HCID 20553328 | — |
| 생성물 | 5-Chloro-3-(3,4-dichlorophenyl)-4-thiazolidinone | HCID 13853453 | — |
반응 단계
3,4-Dichloroaniline was converted to 3-(3,4-dichlorophenyl)-4-thiazolidinone as outlined in Example 1. This thiazolidinone, which had a melting point of 145°-146° C., was chlorinated with thionyl chloride to form 5-chloro-3-(3,4-dichlorophenyl)-4-thiazolidinone having a melting point of 100°-103° C. Recrystallization of this product from ethanol gave 3-(3,4-dichlorophenyl)-5-ethoxy-4-thiazolidinone which had a melting point of 61°-65° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04664694 |
| 출처 데이터셋 | uspto-grants-1987_05 |
| ORD ID | ord-beee820f7b0c4a32aec5ec4e80c04404 |
| 출처 메모 | uspto-grants-1987_05 |