HCID 20201103, 화합물 → 4-Methyl-2-(methylthio)thiophen-3-amine

반응식

[CH3:1][S:2][C:3]1[S:4][CH:5]=[C:6]([CH3:11])[C:7]=1[N+:8]([O-])=O>C(OCC)C>[CH3:1][S:2][C:3]1[S:4][CH:5]=[C:6]([CH3:11])[C:7]=1[NH2:8]

참가 물질

실험 절차

6 g (0.22 gram atoms) freshly prepared aluminium amalgam are added over a period of about two minutes to 18.9 g (0.1 mol) of 2-methylthio-4-methyl-3-nitrothiophene dissolved in 200 ml of moist diethylether. The vigorous reaction which sets in after 5-10 minutes is kept under control by cooling the flask in ice.

후처리

customThe vigorous reaction which
customafter 5-10 minutes
temperatureby cooling the flask in ice

출처 및 근거

ORD 기록: ord-dfa6b5a73c394992a319395e4b4c1656
출처 데이터셋: uspto-grants-1987_05
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04666502

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참가 물질

반응물 1

HCID 20201103HCID 20201103, 화합물

생성물 1

HCID 202011094-Methyl-2-(methylthio)thiophen-3-amine

시약·촉매·용매 1

HCID 3283Diethyl Ether용매

실험 절차

후처리

customThe vigorous reaction which
customafter 5-10 minutes
temperatureby cooling the flask in ice

출처 및 근거

ORD 기록: ord-dfa6b5a73c394992a319395e4b4c1656
출처 데이터셋: uspto-grants-1987_05
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04666502

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불러오는 중…