Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Water → chloromaleic acid N-[2-(2-methoxyphenyl)-ethyl]-imide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | Chloromaleic anhydride | HCID 66772 | — |
| 반응물 | 2-Methoxyphenethylamine | HCID 74896 | — |
| 용매 | Acetic Acid | HCID 176 | — |
| 생성물 | chloromaleic acid N-[2-(2-methoxyphenyl)-ethyl]-imide | HCID 178489456 | 78% |
반응 단계
13.25 g (0.1 mol) of chloromaleic anhydride and 15.2 g (0.1 mol) of 2-(2-methoxyphenyl)-ethylamine are heated to the boiling point in 100 ml of glacial acetic acid for 4 hours. 100 ml of water are then added and the oil which has precipitated is extracted with methylene chloride. The methylene chloride phase is separated off, washed with water, dried and evaporated. The oil which remains crystallizes. 20.8 g (78% of theory) of chloromaleic acid N-[2-(2-methoxyphenyl)-ethyl]-imide are obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04666935 |
| 출처 데이터셋 | uspto-grants-1987_05 |
| ORD ID | ord-33887f723c6e4b00a2adcfa2a364aa5b |
| 출처 메모 | uspto-grants-1987_05 |