Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
p-nitrophenol sodium salt → Tri(4-nitrophenoxy)tri(phenoxy)cyclotriphosphazene
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | p-nitrophenol sodium salt | HCID 13214 | — |
| 반응물 | Trichlorotriphenoxycyclotriphosphazene | HCID 23418754 | — |
| 용매 | Tetrahydrofuran | HCID 8028 | — |
| 생성물 | Tri(4-nitrophenoxy)tri(phenoxy)cyclotriphosphazene | HCID 14274513 | — |
반응 단계
This material is obtained as a white solid by the treatment of sodium and phenol with hexachlorocyclotriphosphazene at -78° C. to produce the trichlorotriphenoxycyclotriphosphazene, according to D. Dell et al., J. Chem. Soc., 4072 (1965), which is incorporated herein by reference. This material is further reacted with sodium 4-nitrophenoxide in refluxing tetrahydrofuran to give the title compound in good yield.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04668589 |
| 출처 데이터셋 | uspto-grants-1987_05 |
| ORD ID | ord-076b72045e604f3193e8079edc061026 |
| 출처 메모 | uspto-grants-1987_05 |