Silane, ethenyltris(1-methylethoxy)- → 1-Tritertbutoxysilyl-2-triisopropoxysilylethylene

HRID 979694

반응식

HRID 979694 반응식
[C:1]([O:5][SiH:6]([O:12][C:13]([CH3:16])([CH3:15])[CH3:14])[O:7][C:8]([CH3:11])([CH3:10])[CH3:9])([CH3:4])([CH3:3])[CH3:2].[CH:17]([Si:19]([O:28][CH:29]([CH3:31])[CH3:30])([O:24][CH:25]([CH3:27])[CH3:26])[O:20][CH:21]([CH3:23])[CH3:22])=[CH2:18]>C1(C)C(C)=CC=CC=1>[C:8]([O:7][Si:6]([O:5][C:1]([CH3:4])([CH3:3])[CH3:2])([O:12][C:13]([CH3:16])([CH3:15])[CH3:14])[CH:18]=[CH:17][Si:19]([O:20][CH:21]([CH3:23])[CH3:22])([O:24][CH:25]([CH3:27])[CH3:26])[O:28][CH:29]([CH3:31])[CH3:30])([CH3:11])([CH3:10])[CH3:9]

참가 물질

4

반응물 2

HCID 87409Silane, ethenyltris(1-methylethoxy)-HCID 101075511Tris(tert-butoxy)silane

생성물 1

HCID 542082861-Tritertbutoxysilyl-2-triisopropoxysilylethylene

시약·촉매·용매 1

HCID 7237O-Xylene용매

반응 조건

온도
225 °C

실험 절차

Into a 45 cc Parr bomb was added 2.5 g (0.010 mol) tritertbutoxysilane, 4.7 g (0.020 mol) vinyltriisopropoxysilane, 1.0 g xylene and 2000 ppm Ru3CO12 (29 mg) as a catalyst. The reaction was heated to 225° C. for 3 hours in a fluidized sand bath. A single product, 1-tritertbutoxysilyl-2-triisopropoxysilylethylene was formed.

출처 및 근거

ORD 기록
ord-ce0c828dc6334923bb02036296c792c4
출처 데이터셋
uspto-grants-1987_05
특허 번호
US04668812

연결된 노트

불러오는 중…