참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Silane, ethenyltris(1-methylethoxy)- | HCID 87409 | — |
| 반응물 | Tris(propan-2-yloxy)silane | HCID 15722916 | — |
| 용매 | O-Xylene | HCID 7237 | — |
| 생성물 | 1,2-Bis(triisopropoxysilyl)ethylene | HCID 53828948 | — |
반응 단계
Into a 45 cc Parr bomb was added 2.5 g (0.012 mol) triisopropoxysilane, 5.7 g (0.024 mol) vinyltriisopropoxysilane, 1.0 xylene and 200 ppm Ru3CO12 (20 mg). The reaction was heated for 4 hours at 225° C. in a fluidized sand bath. A single product, 1,2-bis(triisopropoxysilyl)ethylene was formed.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04668812 |
|---|
| 출처 데이터셋 | uspto-grants-1987_05 |
|---|
| ORD ID | ord-1cfea45e05b949b0bff2e9a9f1f49b20 |
|---|
| 출처 메모 | uspto-grants-1987_05 |
|---|
