Triethylamine → Chromium (II) bis(2-ethylhexanoate)

반응식

C(N(CC)CC)C.[CH2:8]([CH:10]([CH2:14][CH2:15][CH2:16][CH3:17])[C:11]([OH:13])=[O:12])[CH3:9].[Cl-].[Cr+2:19].[Cl-]>CCCCCCC>[CH2:8]([CH:10]([CH2:14][CH2:15][CH2:16][CH3:17])[C:11]([O-:13])=[O:12])[CH3:9].[CH2:8]([CH:10]([CH2:14][CH2:15][CH2:16][CH3:17])[C:11]([O-:13])=[O:12])[CH3:9].[Cr+2:19]

참가 물질

실험 절차

Chromium (II) bis(2-ethylhexanoate) is prepared by the addition of an equimolar mixture of triethylamine and 2-ethylhexanoic acid in heptane to a suspension of 0.5 mole anhydrous chromium (II) chloride in heptane. A slow reaction results in the formation of a deep purple solution and the precipitation of triethylammonium hydrochloride. The product is isolated as a purple oil after removal of the precipitate by filtration and the volatiles under vacuum.