Hydrogen Peroxide → Hydrogen Peroxide

HRID 979747

반응식

HRID 979747 반응식
[C:1]([NH:14][CH2:15][C:16]([OH:18])=[O:17])(=[O:13])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12].[OH:19][OH:20]>CS(O)(=O)=O>[C:1]([NH:14][CH2:15][C:16]([OH:18])=[O:17])(=[O:13])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12].[OH:19][OH:20].[C:1]([NH:14][CH2:15][C:16]([O:18][OH:19])=[O:17])(=[O:13])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12]

참가 물질

6

반응물 2

HCID 784Hydrogen PeroxideHCID 346152N-Lauroylglycine

생성물 3

HCID 784Hydrogen PeroxideHCID 346152N-LauroylglycineHCID 54133591N-lauroylaminoperoxyacetic acid

시약·촉매·용매 1

HCID 6395Methanesulfonic Acid용매2회

실험 절차

N-Lauroylaminoperoxyacetic acid was prepared by reaction of N-lauroylglycine with hydrogen peroxide in methanesulfonic acid according to the procedure described in Example II. From 50.0 g (0.195 mol) of N-lauroylglycine and 33.1 g (0.973 mol) of hydrogen peroxide in 100 mL methanesulfonic acid was obtained 38.0 g of N-lauroylaminoperoxyacetic acid having an AvO of 3.03% (theoretical yield=53.2 g having an AvO of 5.86%).

출처 및 근거

ORD 기록
ord-c28cded40e394c00b11c9f23f9f09404
출처 데이터셋
uspto-grants-1987_01
특허 번호
US04634551

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