Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ammonia → 2-{Bicyclo[2.2.1]heptan-2-yl}ethan-1-amine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ammonia | HCID 222 | — |
| 반응물 | Thionyl Chloride | HCID 24386 | — |
| 반응물 | Norborn-2-ylacetic acid | HCID 79139 | — |
| 반응물 | Aluminium lithium hydride | HCID 21226445 | — |
| 생성물 | 2-{Bicyclo[2.2.1]heptan-2-yl}ethan-1-amine | HCID 20222870 | 35% |
반응 단계
Norbornane-2-acetic acid was treated with SOCl2, then with NH3. The resulting amine was reduced with LiAlH4 to give the desired intermediate. Yield: 35%.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04634701 |
| 출처 데이터셋 | uspto-grants-1987_01 |
| ORD ID | ord-89ff04e69db24ab5aa91db85b2fdded3 |
| 출처 메모 | uspto-grants-1987_01 |