Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methanol → 6-(Methoxycarbonyl)pyridine-2-carboxylic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methanol | HCID 887 | — |
| 반응물 | Sulfuric Acid | HCID 1118 | — |
| 반응물 | 2,6-Pyridinedicarboxylic acid, 1-oxide | HCID 85179 | — |
| 생성물 | 6-(Methoxycarbonyl)pyridine-2-carboxylic acid | HCID 4019172 | — |
반응 단계
40 g of the pyridine-2,6-dicarboxylic acid N-oxide was dissolved in 100 ml of methanol. 5 ml of sulfuric acid was added to the solution. The admixture was then heated under reflux for 2 hours and allowed, to cool so that crystals were deposited. The crystals thus deposited were filtered to obtain 28 g of 6-methoxycarbonylpyridine-2-carboxylic acid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04636462 |
| 출처 데이터셋 | uspto-grants-1987_01 |
| ORD ID | ord-9d7fec5c60514ea085ebc787b0ee6e21 |
| 출처 메모 | uspto-grants-1987_01 |