참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Phloroglucinol | HCID 359 | — |
| 반응물 | Dimethylformamide | HCID 6228 | — |
| 반응물 | Phosphorus oxychloride | HCID 24813 | — |
| 반응물 | 1,4-Dioxane | HCID 31275 | — |
| 생성물 | 2,4-Dimethyl-1,3,5-benzenetriol | HCID 78214 | — |
반응 단계
0.6 kg of phloroglucinol is dissolved in 1.4 liters of dioxan and a mixture containing 0.8 liters of N,N-dimethylformamide and 0.96 liters of phosphorus oxychloride is added slowly and with vigorous stirring. The addition of the reagent having been completed, the reaction is maintained at 40° C. for 12 hours containing the stirring and then the whole is poured over 10 kg of crushed ice.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04636569 |
|---|
| 출처 데이터셋 | uspto-grants-1987_01 |
|---|
| ORD ID | ord-95c952b9479f46159281fca5ca64d23e |
|---|
| 출처 메모 | uspto-grants-1987_01 |
|---|
