Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydroxyacetonitrile → (Dodecylamino)acetonitrile
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydroxyacetonitrile | HCID 7857 | — |
| 반응물 | Dodecylamine | HCID 13583 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | (Dodecylamino)acetonitrile | HCID 222308 | — |
반응 단계
In a flask of 500 ml provided with a magnetic stirrer, 4.56 gr of hydroxyacetonitrile (0.08 mol) were mixed at room temperature with 16.3 gr of dodecylamine (0.088 mol) in 250 ml of methanol. The mixture was allowed to stand for 16 hours at room temperature and methanol was evaporated. The obtained liquid was distilled under 10-2 mm Hg. The fraction distilling between 106° and 116° crystallizes after cooling.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04639468 |
| 출처 데이터셋 | uspto-grants-1987_01 |
| ORD ID | ord-062b5b872d41428695569fdb5abf608a |
| 출처 메모 | uspto-grants-1987_01 |