Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acetic Acid → Phenoxybutylamine acetate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acetic Acid | HCID 176 | — |
| 반응물 | Butyl isocyanide | HCID 76008 | — |
| 반응물 | 4-Phenoxybutan-1-amine | HCID 116240 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | Phenoxybutylamine acetate | HCID 70062463 | — |
반응 단계
In a three-necked flask of 25 ml provided with a magnetic bar, a calcium chloride tube and a dropping funnel, 1.99 gr (0.012 mol) of phenoxybutylamine, 1 gr (0.012 mol) of n-butylisonitrile and 0.72 gr of acetic acid were mixed in 5 ml of methanol. A precipitate of phenoxybutylamine acetate formed. This suspension cooled in an ice bath was added under good agitation with 0.87 gr (0.012 mol) of isobutyraldehyde.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04639468 |
| 출처 데이터셋 | uspto-grants-1987_01 |
| ORD ID | ord-6736ed9f75254637a52481ecc0d7be4d |
| 출처 메모 | uspto-grants-1987_01 |