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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 981258생성일: 2026년 10월 27일

Lauroyl peroxide → Furan-2,5-dione--methoxyethene (1/1)

https://huagongshe.com/reaction/981258

반응식

참여 물질

역할이름HCID투입량
반응물Lauroyl peroxideHCID 7773—
반응물Maleic AnhydrideHCID 7923—
생성물Furan-2,5-dione--methoxyethene (1/1)HCID 62708—

반응 조건

온도55 °C

반응 단계

87.3 g of maleic anhydride and 1.46 g of dilauroyl peroxide were introduced into a 2 1 Juchheim pressurized reaction vessel, and the reaction apparatus was then flushed with nitrogen. When the apparatus was free from oxygen, 310 g of methyl vinyl ether which had been dried over solid sodium hydroxide and freshly distilled, were added. The reaction mixture was warmed to 55° C. with stirring and maintained at this temperature for 2 hours under pressure. After the mixture had cooled to 20° C., excess methyl vinyl ether was distilled off, and the reaction product was removed from the vessel. This gave 118 g (84.9 % of theory) of an MA/MVE copolymer having the following properties: loss on drying at 105° C.: 0.92 %, at 60° C. in vacuo: 0.25 %. The particle size distribution, which was measured by sieve analysis, gave the following values:

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US04990551
출처 데이터셋uspto-grants-1991_02
ORD IDord-11597619b51248b3af52dce2b18efef4
출처 메모uspto-grants-1991_02