참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Lauroyl peroxide | HCID 7773 | — |
| 반응물 | Maleic Anhydride | HCID 7923 | — |
| 생성물 | Furan-2,5-dione--methoxyethene (1/1) | HCID 62708 | — |
반응 단계
87.3 g of maleic anhydride and 1.46 g of dilauroyl peroxide were introduced into a 2 1 Juchheim pressurized reaction vessel, and the reaction apparatus was then flushed with nitrogen. When the apparatus was free from oxygen, 310 g of methyl vinyl ether which had been dried over solid sodium hydroxide and freshly distilled, were added. The reaction mixture was warmed to 55° C. with stirring and maintained at this temperature for 2 hours under pressure. After the mixture had cooled to 20° C., excess methyl vinyl ether was distilled off, and the reaction product was removed from the vessel. This gave 118 g (84.9 % of theory) of an MA/MVE copolymer having the following properties: loss on drying at 105° C.: 0.92 %, at 60° C. in vacuo: 0.25 %. The particle size distribution, which was measured by sieve analysis, gave the following values:
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 특허 번호 | US04990551 |
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| 출처 데이터셋 | uspto-grants-1991_02 |
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| ORD ID | ord-11597619b51248b3af52dce2b18efef4 |
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| 출처 메모 | uspto-grants-1991_02 |
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