Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
p-Toluenesulfonic acid → Ditridecyl 2-bromosuccinate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | p-Toluenesulfonic acid | HCID 6101 | — |
| 반응물 | 1-Tridecanol | HCID 8207 | — |
| 반응물 | Bromosuccinic acid | HCID 73557 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | Ditridecyl 2-bromosuccinate | HCID 20072149 | — |
반응 단계
A mixture of 19.7 g. (0.1 mole) of bromosuccinic acid, 40.1 g. (0.2 mole) of tridecanol, 0.25 g. of p-toluenesulfonic acid and 200 ml. of toluene is refluxed for 7 hours, using a Dean-Stark trap. There is collected 3.6 ml. of H2O in the trap which is exactly the calculated amount for this reaction when completed.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04990652 |
| 출처 데이터셋 | uspto-grants-1991_02 |
| ORD ID | ord-d8480f33bd4548e6902f13e99b1fd1c8 |
| 출처 메모 | uspto-grants-1991_02 |