Isobutylbenzene → 4'-Isobutylacetophenone

HRID 981373

반응식

HRID 981373 반응식
[CH2:1]([C:5]1[CH:10]=[CH:9][CH:8]=[CH:7][CH:6]=1)[CH:2]([CH3:4])[CH3:3].[C:11](F)(=[O:13])[CH3:12]>CC(O)=O>[CH3:3][CH:2]([CH2:1][C:5]1[CH:10]=[CH:9][C:8]([C:11]([CH3:12])=[O:13])=[CH:7][CH:6]=1)[CH3:4]

참가 물질

4

반응물 2

HCID 10870IsobutylbenzeneHCID 11204Acetyl fluoride

생성물 1

HCID 932144'-Isobutylacetophenone

시약·촉매·용매 1

HCID 176Acetic Acid용매

실험 절차

Isobutylbenzene (IBB) (10.2 lb/hr) and a solution of HF containing 13 wt % HOAc and 12 wt % acetyl fluoride (AcF) (153 lb/hr) were fed into reactor 1 through line 4. The mixture was reacted at 60° C. for 1.5 hrs to produce the desired 4-isobutylacetophenone product.

후처리

  1. customwere fed into reactor
  2. customThe mixture was reacted at 60° C. for 1.5 hrs

출처 및 근거

ORD 기록
ord-d3b93062aae846dd972c13f70c9a7b8b
출처 데이터셋
uspto-grants-1991_02
특허 번호
US04990681

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