Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Water → HCID 19824186, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | Dichloromethane | HCID 6344 | — |
| 반응물 | Hexane | HCID 8058 | — |
| 반응물 | Phenol, 2,6-bis(1,1-dimethylethyl)-4-nitroso- | HCID 70383 | — |
| 반응물 | HCID 178418361 | HCID 178418361 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 생성물 | HCID 19824186 | HCID 19824186 | — |
반응 단계
A 2 liter Parr bomb was charged with 210.5 g of 44.6% water wet (0.5 mole, pure, dry) 2,6-di-tert-butyl-4-nitrosophenol, 2.0 g of 5% Pd/C catalyst, 300 ml dichloromethane and 400 ml hexane. The nitrogen purged system was pressurized to 50 psi with hydrogen and the rate of hydrogen uptake noted. Hydrogenation was completed within one hour.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04990671 |
| 출처 데이터셋 | uspto-grants-1991_02 |
| ORD ID | ord-89e4a46da6b64ab080f7764d88a2ecde |
| 출처 메모 | uspto-grants-1991_02 |