HCID 20070371, 화합물 → 1-Propanol, 2-[(2-aminophenyl)amino]-2-methyl-
반응식
[CH3:1][C:2]([NH:6][C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][C:8]=1[N+:13]([O-])=O)([CH3:5])[CH2:3][OH:4]>C(O)C.[Pd]>[CH3:5][C:2]([NH:6][C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][C:8]=1[NH2:13])([CH3:1])[CH2:3][OH:4]참가 물질
4
실험 절차
2-(1,1-dimethyl-2-hydroxyethyl)aminonitrobenzene (10 g) in ethanol (200 ml) was hydrogenated at 50p.s.i. (345 kPa) over 5% Pd/C (0.5 g) for 2 hours. The catalyst was filtered off and the solvent removed under reduced pressure yielding the title compound as a yellow foam 8.4 g (98%).
후처리
- filtrationThe catalyst was filtered off
- customthe solvent removed under reduced pressure
출처 및 근거
- ORD 기록
- ord-cdeb9fdeb99742dfa3c8a0d9568cd911
- 출처 데이터셋
- uspto-grants-1991_02
- 특허 번호
- US04992447
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