Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
8-Aminooctanoic acid → HCID 178512800, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 8-Aminooctanoic acid | HCID 66085 | — |
| 반응물 | Diisopropylethylamine | HCID 81531 | — |
| 반응물 | 3,5-Dimethylpyrazole-1-carboxamidine | HCID 97525 | — |
| 용매 | Water | HCID 962 | — |
| 용매 | 1,4-Dioxane | HCID 31275 | — |
| 생성물 | HCID 178512800 | HCID 178512800 | — |
반응 단계
3,5-dimethyl-pyrazole-1-carboxamidine (100 g; 0.5 Mole) and N,N-diisopropylethyl amine (DIEA) (65 g; 0.5 Mole) were suspended in dioxane (300 ml) and water (115 ml). 8-Amino-octanoic acid (48 g; 0.3 Mole) was added to the mixture with stirring. The colorless solution was then refluxed for 2 days. The product was filtered and washed with water (3 x 50 ml).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04992463 |
| 출처 데이터셋 | uspto-grants-1991_02 |
| ORD ID | ord-1b9699da9c8b44078c0bcf02bf7c4c79 |
| 출처 메모 | uspto-grants-1991_02 |