Acetyl chloride → HCID 20069224, 화합물

HRID 982151노트

반응식

[C:1]1([CH:7]([C:9]2[CH:14]=[CH:13][CH:12]=[CH:11][C:10]=2[CH:15]=[CH2:16])[CH3:8])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.C1(C(C2C=CC=CC=2)C)C=CC=CC=1.C(Cl)(=[O:33])C>>[C:1]1([CH:7]([C:9]2[CH:14]=[CH:13][CH:12]=[CH:11][C:10]=2[C:15](=[O:33])[CH3:16])[CH3:8])[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1

참가 물질

반응물 3

HCID 6367Acetyl chloride

HCID 119181,1-Diphenylethane

HCID 21696373HCID 21696373, 화합물

생성물 1

HCID 20069224HCID 20069224, 화합물

실험 절차

They can be prepared by a variety of chemical synthetic manners, and for example, phenyl-(vinylpheny)ethane may be prepared by reacting diphenylethane with acetyl chloride in the presence of a Friedel-Crafts catalyst to form phenyl(acetylphenyl)ethane, reducing the latter with sodium boron hydrine or the like, and dehydrating it. Phenyl(isopropenylphenyl)ethane can be prepared by reacting phenyl(formylphenyl)ethane with a Grignard reagent such as methylmagnesium iodide, and carrying out dehydration.

후처리

customThey can be prepared by a variety of chemical synthetic manners

출처 및 근거

ORD 기록: ord-c89ac98360e843c99d77f82aa1d105c1
출처 데이터셋: uspto-grants-1991_02
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04994539

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