Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Thionyl Chloride → 2-[(Phenylmethyl)thio]benzoyl chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Thionyl Chloride | HCID 24386 | — |
| 반응물 | 2-(Benzylsulfanyl)benzoic acid | HCID 264182 | — |
| 용매 | Benzene | HCID 241 | — |
| 생성물 | 2-[(Phenylmethyl)thio]benzoyl chloride | HCID 20067340 | 94.1% |
반응 단계
A suspension of 100 g of 2-[(phenylmethyl)thio]benzoic acid and 97.6 g of thionyl chloride in 800 ml of benzene was refluxed for about three hours then evaporated to dryness under vacuum. The residue was triturated with hexane to yield 101.2 g of 2-[(phenylmethyl)thio]benzoyl chloride, m.p. 113° to 116° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04995901 |
| 출처 데이터셋 | uspto-grants-1991_02 |
| ORD ID | ord-f6ab892768b743d48204bed41050d080 |
| 출처 메모 | uspto-grants-1991_02 |