Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3-Phenylprop-2-Enal → 1,2-Diphenyl-1-(4-benzyloxyphenyl)butane-1,4-diol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3-Phenylprop-2-Enal | HCID 307 | — |
| 반응물 | 4-Benzyloxybenzophenone | HCID 458193 | — |
| 생성물 | 1,2-Diphenyl-1-(4-benzyloxyphenyl)butane-1,4-diol | HCID 20067707 | — |
반응 단계
The (RR,SS; RS,SR)-isomer mixture is prepared from 13.2 g of cinnamaldehyde and 28.8 g of 4-benzyloxybenzophenone according to the procedure described in Example 9. Recrystallization is performed from toluene. The yield is 32.5 g (77%) of a product having m.p. 109°-15° C. The product contains both isomer pairs (RR,SS: RS,SR 1:1).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04996225 |
| 출처 데이터셋 | uspto-grants-1991_02 |
| ORD ID | ord-ef7c29f058d74ec0800ee44b30bb37e6 |
| 출처 메모 | uspto-grants-1991_02 |