Acetone → 2,6-Dihydroxynaphthalene

반응식

[CH3:1][C:2]([CH3:4])=[O:3].[CH3:5][CH:6]([CH2:8][C:9]([CH3:11])=[O:10])[CH3:7].[CH3:12]C(C)=O>>[OH:3][C:2]1[CH:4]=[CH:7][C:6]2[C:5](=[CH:12][CH:11]=[C:9]([OH:10])[CH:8]=2)[CH:1]=1

참가 물질

반응물 2

HCID 180Acetone

HCID 18671121MIBK acetone

생성물 1

HCID 935522,6-Dihydroxynaphthalene

실험 절차

Sixty parts by weight of acetone was added to 100 parts by weight of the oily phase containing the oxidation product obtained in Example 8, (1) to prepare an MIBK/acetone mixed oily phase which was subjected to acid cleavage by the following method to obtain 2,6-dihydroxynaphthalene.

출처 및 근거

ORD 기록: ord-c8d800a2a68e4214a68488536c41fcff
출처 데이터셋: uspto-grants-1991_02
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04996372

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