Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Diethylenetriamine → 2,2,2-trifluoro-N-[2-[2-[(2,2,2-trifluoroacetyl)amino]ethylamino]ethyl]acetamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Diethylenetriamine | HCID 8111 | — |
| 반응물 | Ethyl trifluoroacetate | HCID 9794 | — |
| 용매 | Tetrahydrofuran | HCID 8028 | — |
| 생성물 | 2,2,2-trifluoro-N-[2-[2-[(2,2,2-trifluoroacetyl)amino]ethylamino]ethyl]acetamide | HCID 388778 | — |
반응 단계
113.3 g (790 mmol) of trifluoroacetic acid ethyl ester is added in drops to a solution consisting of 41.14 g (390 mmol) of 1,4,7-triazaheptane in 350 ml of tetrahydrofuran at 80° C. and under nitrogen. It is allowed to stir overnight at room temperature, concentrated by evaporation in a vacuum. The remaining oil is crystallized from hexane.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06861043B2 |
| 출처 데이터셋 | uspto-grants-2005_03 |
| ORD ID | ord-b1d80b98d6be4a1a84c54c7f8f1f3480 |
| 출처 메모 | uspto-grants-2005_03 |