Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Benzyl Alcohol → 2-(Benzyloxy)benzyl-triphenylphosphonium bromide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Benzyl Alcohol | HCID 244 | — |
| 반응물 | Triphenylphosphonium hydrobromide | HCID 22178555 | — |
| 용매 | Acetonitrile | HCID 6342 | — |
| 생성물 | 2-(Benzyloxy)benzyl-triphenylphosphonium bromide | HCID 11410109 | — |
반응 단계
15.15 g (70.7 mmol) of the benzyl alcohol IIIa and 21.86 g (63.7 mmol) of triphenyl-phosphonium hydrobromide in 240 ml of acetonitrile are heated at reflux for 5 hours. The solvent is evaporated under reduced pressure, and diethyl ether is then added. The solid is filtered and dried under reduced pressure.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06864287B1 |
| 출처 데이터셋 | uspto-grants-2005_03 |
| ORD ID | ord-386711396fe54941b2746e6a44162c3f |
| 출처 메모 | uspto-grants-2005_03 |