Thionyl Chloride → HCID 22557298, 화합물
반응식
[O:1]=[C:2]1[NH:7][N:6]=[C:5]([C:8]2[CH:16]=[CH:15][C:11]([C:12](O)=[O:13])=[CH:10][CH:9]=2)[CH2:4][CH2:3]1.S(Cl)([Cl:19])=O>ClCCl>[O:1]=[C:2]1[NH:7][N:6]=[C:5]([C:8]2[CH:16]=[CH:15][C:11]([C:12]([Cl:19])=[O:13])=[CH:10][CH:9]=2)[CH2:4][CH2:3]1참가 물질
4
실험 절차
10 mmol (2.2 g) of 4-(1,4,5,6-tetrahydro-6-oxo-3-pyridazinyl)benzoic acid are suspended in 50 ml of dichloromethane, after which 1.5 ml (20 mmol) of thionyl chloride are added and the mixture is stirred for 24 hours while being boiled gently.
출처 및 근거
- ORD 기록
- ord-289c455c455f441f9a3cb3f6ba415f23
- 출처 데이터셋
- uspto-grants-2005_03
- 특허 번호
- US06867206B1
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