2,4-Dichlorobenzylidenemalononitrile → HCID 10288085, 화합물

반응식

[CH:1]1[C:9]2[C:8]3[CH:10]=[CH:11][CH:12]=[CH:13][C:7]=3[O:6][C:5]=2[CH:4]=[CH:3][C:2]=1[C:14]([NH2:16])=[NH:15].[Cl:17][C:18]1[CH:29]=[C:28]([Cl:30])[CH:27]=[CH:26][C:19]=1[CH:20]=[C:21]([C:24]#[N:25])[C:22]#[N:23]>>[NH2:25][CH2:24][C:21]1[C:22]([NH2:23])=[N:15][C:14]([C:2]2[CH:3]=[CH:4][C:5]3[O:6][C:7]4[CH:13]=[CH:12][CH:11]=[CH:10][C:8]=4[C:9]=3[CH:1]=2)=[N:16][C:20]=1[C:19]1[CH:26]=[CH:27][C:28]([Cl:30])=[CH:29][C:18]=1[Cl:17]

참가 물질

반응물 2

HCID 180892,4-Dichlorobenzylidenemalononitrile

HCID 22220613HCID 22220613, 화합물

생성물 1

HCID 10288085HCID 10288085, 화합물

실험 절차

The title compound, MS: m/e=434.9 (M+), was prepared from dibenzofuran-2-carboxamidine and 2-(2,4-dichloro-benzylidene)-malononitrile in analogy to the process described in Example 11 as a solid.

출처 및 근거

ORD 기록: ord-0a1be1300f90420e9cd41ddd7104eabf
출처 데이터셋: uspto-grants-2005_03
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US06867205B2

반응 노트

불러오는 중…