2-(Bromomethyl)benzonitrile → HCID 22508571, 화합물

HRID 984828노트

반응식

HRID 984828 반응식
[Br:1][C:2]1[N:10]([CH2:11][C:12]2[CH:17]=[CH:16][CH:15]=[CH:14][C:13]=2[Cl:18])[C:9]2[C:8](=[O:19])[NH:7][C:6](=[O:20])[N:5]([CH3:21])[C:4]=2[N:3]=1.Br[CH2:23][C:24]1[C:25]([C:30]#[N:31])=[CH:26][CH:27]=[CH:28][CH:29]=1>>[Br:1][C:2]1[N:10]([CH2:11][C:12]2[CH:17]=[CH:16][CH:15]=[CH:14][C:13]=2[Cl:18])[C:9]2[C:8](=[O:19])[N:7]([CH2:23][C:24]3[CH:29]=[CH:28][CH:27]=[CH:26][C:25]=3[C:30]#[N:31])[C:6](=[O:20])[N:5]([CH3:21])[C:4]=2[N:3]=1

참가 물질

3

반응물 2

HCID 895992-(Bromomethyl)benzonitrileHCID 6496888-Bromo-7-(2-chloro-benzyl)-3-methyl-3,7-dihydro-purine-2,6-dione

생성물 1

HCID 22508571HCID 22508571, 화합물

실험 절차

8-Bromo-7-(2-chlorobenzyl)-3-methyl-3,7-dihydropurine-2,6-dione (75A) and alpha-bromo-o-tolunitrile were reacted and purified as described in the General procedure G, Step B, to afford 75B as white crystals.

후처리

  1. custompurified

출처 및 근거

ORD 기록
ord-8f25fb3668db4b22b89be73cfab14aeb
출처 데이터셋
uspto-grants-2005_03
특허 번호
US06869947B2

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