Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4,4-Dimethyl-2-(2-methoxyphenyl)oxazoline → 2-(3,5-Dichloro-4'-fluoro-2-[1,1'-biphenyl]yl)-4,4-dimethyl-2-oxazoline
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4,4-Dimethyl-2-(2-methoxyphenyl)oxazoline | HCID 333189 | — |
| 반응물 | 2-(2,4-Dichloro-6-methoxyphenyl)-4,4-dimethyl-2-oxazoline | HCID 12802883 | — |
| 반응물 | HCID 178418676 | HCID 178418676 | — |
| 반응물 | HCID 178489560 | HCID 178489560 | — |
| 생성물 | 2-(3,5-Dichloro-4'-fluoro-2-[1,1'-biphenyl]yl)-4,4-dimethyl-2-oxazoline | HCID 12802884 | — |
반응 단계
By substituting equimolar amounts of 2-(2,4-dichloro-6-methoxyphenyl)-4,4-dimethyl-2-oxazoline and 4-fluorophenylmagnesium bromide for 2-(2-methoxyphenyl)-4,4-dimethyl-2-oxazoline and 2-methoxyphenylmagnesium bromide, the title compound was prepared following the procedure of Example 17, Step A, (85%), mp 93°-95° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04710513 |
| 출처 데이터셋 | uspto-grants-1987_12 |
| ORD ID | ord-f8a353aafcc1481e86df9107b4a806d0 |
| 출처 메모 | uspto-grants-1987_12 |