Isoprene → HCID 15664015, 화합물

HRID 986686노트

반응식

HRID 986686 반응식
[C:1]1([CH3:9])[C:2]([NH2:8])=[CH:3][CH:4]=[CH:5][C:6]=1[NH2:7].[CH2:10]=[CH:11][C:12](=[CH2:14])[CH3:13].CCCCC>>[CH3:13][C:12]([CH3:14])=[CH:11][CH2:10][C:3]1[CH:4]=[CH:5][C:6]([NH2:7])=[C:1]([CH3:9])[C:2]=1[NH2:8]

참가 물질

4

반응물 3

HCID 6557IsopreneHCID 8003PentaneHCID 132052,6-Diaminotoluene

생성물 1

HCID 15664015HCID 15664015, 화합물

실험 절차

A 200 g (1.64 mol) portion of 2,6-toluenediamine, 167 g (2.45 mol) of isoprene, 200 g (2.78 mol) of pentane, and 20 g of powdered H-Y zeolite were reacted at 150° C. in a similar fashion as indicated in Example 1. Isolation of a catalyst free sample was obtained by hot filtration. Selective removal of all residual hydrocarbon by vacuum distillation afforded the following product mixture:

후처리

  1. customIsolation of a catalyst free sample was obtained by hot filtration
  2. customremoval of all residual hydrocarbon
  3. distillationby vacuum distillation
  4. customafforded the following product mixture

출처 및 근거

ORD 기록
ord-d0e0d84d3b524999bc081a476fe80962
출처 데이터셋
uspto-grants-1987_12
특허 번호
US04714778

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