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Sodium Carbonate → Tricalcium Phosphate

HRID 986879
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HRID 986879 반응식
S([O-])([O-])(=O)=O.[Al+3].S([O-])([O-])(=O)=O.S([O-])([O-])(=O)=O.[Al+3].C(=O)([O-])[O-].[Na+].[Na+].[O-:24][P:25]([O:28]P([O-])([O-])=O)(=[O:27])[O-:26].[Ca+2:33].[Ca+2]>>[P:25]([O-:28])([O-:27])([O-:26])=[O:24].[Ca+2:33].[P:25]([O-:28])([O-:27])([O-:26])=[O:24].[Ca+2:33].[Ca+2:33]
참가 물질실험 절차후처리출처 및 근거반응 노트

참가 물질

4

반응물 3

HCID 10340Sodium CarbonateHCID 24632Calcium pyrophosphate (Ca2P2O7)HCID 24850Aluminum Sulfate

생성물 1

HCID 24456Tricalcium Phosphate

실험 절차

In this method, the first reactant, 800 g of a 12% aqueous solution of aluminum sulfate was added to the reactor vessel, then the second reactant, an 18% aqueous solution of sodium carbonate, was metered into the vessel at a rate of 7 ml/minute until the pH reached 5.9. The reactants were mixed together for 20 minutes under agitation. Next, 54 grams of calcium pyrophosphate was added and the resulting slurry was mixed for 15 minutes with agitation and filtered and washed to a conductivity of about 2000 μmhos. The recovered wetcake was reslurried with 150 g of water and 200 g of a 1% FD&C Blue No. 1 aqueous solution to form a slurry of colored calcium phosphate colorant and this slurry was then mixed for approximately 1 hour.

후처리

  1. additionThe reactants were mixed together for 20 minutes under agitation
  2. additionthe resulting slurry was mixed for 15 minutes with agitation
  3. filtrationfiltered
  4. washwashed to a conductivity of about 2000 μmhos

출처 및 근거

ORD 기록
ord-a225f7a185e74e02bae100a1e0f1e151
출처 데이터셋
uspto-grants-2003_10
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US06630019B2

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