Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3-(4-Benzyloxy-3-methoxyphenyl)-2-ethoxyacrylic acid ethyl ester → 3-(4-Benzyloxy-3-methoxyphenyl)-2-ethoxypropanoic acid ethyl ester
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3-(4-Benzyloxy-3-methoxyphenyl)-2-ethoxyacrylic acid ethyl ester | HCID 53757958 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 용매 | Ethyl Acetate | HCID 8857 | — |
| 생성물 | 3-(4-Benzyloxy-3-methoxyphenyl)-2-ethoxypropanoic acid ethyl ester | HCID 54162019 | 97% |
반응 단계
3-(4-Benzyloxy-3-methoxyphenyl)-2-ethoxyacrylic acid ethyl ester (5.5 g, 15.4 mmole) was dissolved in ethyl acetate and hydrogenated using Pd/C (dry, 5%). The reaction mixture was filtered through celite. Evaporation of the filtrate gave 4 g (97% yield) of 3-(4-benzyloxy-3-methoxyphenyl)-2-ethoxypropanoic acid ethyl ester.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06630600B1 |
| 출처 데이터셋 | uspto-grants-2003_10 |
| ORD ID | ord-643d5dcc0cdc4665afdff22b52cc4807 |
| 출처 메모 | uspto-grants-2003_10 |